Synthesis of Biodegradable Polymer Scaffolds

Glycerol, 4-dimethylaminopyridine and triethylamine were obtained from Fisher Scientific (Loughborough, Leicestershire, UK). Sebacic acid was obtained from Alfa Aesar (Ward Hill, MA, USA). Dichloromethane, polyethylene glycol (M_w 8000), stannous octanoate, p-toluenesulfonic acid monohydrate, lactic acid (85%), polycaprolactone (M_w 80,000), 1,1,1,3,3,3-hexafluoro-2-propanol (HFIP), polyethylene glycol diacrylate (M_w 8000) (PEGDA₈₀₀₀), 2-hydroxy-4′-(2-hydroxyethoxy)-2-methylpropiophenone (Irgacure 2959) and anhydrous magnesium sulphate (MgSO₄) were obtained from Sigma Aldrich (Burlington, MA, USA).

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Phillips M., Tronci G., Pask C.M, & Russell S.J. (2024). Nonwoven Reinforced Photocurable Poly(glycerol sebacate)-Based Hydrogels. Polymers, 16(7), 869.

Publication 2024

Glycerol 4-dimethylaminopyridine triethylamine Sebacic acid Dichloromethane p-toluenesulfonic acid monohydrate 2-hydroxy-4′-(2-hydroxyethoxy)-2-methylpropiophenone (Irgacure 2959) anhydrous magnesium sulphate (MgSO4)

Corresponding Organization :

Other organizations : University of Leeds

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Variable analysis

independent variables

Glycerol
4-dimethylaminopyridine
Triethylamine
Sebacic acid
Dichloromethane
Polyethylene glycol (M_w 8000)
Stannous octanoate
P-Toluenesulfonic acid monohydrate
Lactic acid (85%)
Polycaprolactone (M_w 80,000)
1,1,1,3,3,3-Hexafluoro-2-propanol (HFIP)
Polyethylene glycol diacrylate (M_w 8000) (PEGDA_8000)
2-Hydroxy-4'-(2-hydroxyethoxy)-2-methylpropiophenone (Irgacure 2959)
Anhydrous magnesium sulphate (MgSO_4)

dependent variables

Not explicitly mentioned

control variables

Not explicitly mentioned

positive controls

Not specified

negative controls

Not specified

Annotations

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