FTIR spectra for GO and SGO composite membranes were taken using a Perkin Elmer FTIR spectrometer (Waltham, MA, USA). The morphological features (i.e., top surface and membrane microstructures) of the prepared membranes were characterized using SEM (FEI, Quanta FEG 450, Thermo Scientific, Waltham, MA, USA). The crystalline structure of prepared SGO doped CA membranes was characterized through X-ray diffraction (PANalytical X’pert, Malvern Panalytical, Malvern, UK) technique, respectively.
Thermal properties of SGO doped composite membranes were determined using differential scanning calorimetry (DSC-250, TA instruments, New Castle, DE, USA) at a 10 °C/min heating rate under nitrogen flow of 30 mL/min. Ten milligram samples were sealed in an aluminum pan and scanned over a range of 25 °C to 500 °C [28 (link)].
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