Immunogold Labeling of Nsp1 Protein
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Corresponding Organization : Tokyo Institute of Technology
Other organizations : Yokohama City University, Yokohama City University Medical Center
Variable analysis
- Rapid freezing and freeze-fixation methods
- Freezing of cells sandwiched with copper disks in liquid propane at -175°C
- Substitution with 1% tannic acid in ethanol and 2% distilled water at -80°C for 48 h, then -20°C for 4 h and 4°C for 1 h
- Dehydration in anhydrous ethanol for 30 min three times
- Infiltration with a 50:50 mixture of ethanol and LR white resin at 4°C for 1 h
- Washing with LR white three times by incubation at 4°C for 30 min each
- Polymerization of resin at 50°C overnight
- Immunostaining of ultrathin sections with anti-Nsp1 antibodies and 10-nm gold particle-conjugated secondary antibodies
- Electron microscopy using a transmission electron microscope (JEM-1400Plus; JEOL) and digital image capture (3,296 × 2,472 pixels) using a charge-coupled device camera (EM-14830RUBY2; JEOL)
- Temperature: -175°C, -80°C, -20°C, 4°C, 50°C
- Reagents: 1% tannic acid in ethanol, 2% distilled water, anhydrous ethanol, LR white resin
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