Synthesis and Characterization of Fluorinated Polymeric Compounds

Example 1

Compound (3A) was obtained with reference to the method for producing compound (ii-2) described in WO2014/126064.
CF₃ CF₂—OCF₂ CF₂—(OCF₂ CF₂ CF₂ CF₂ OCF₂ CF₂)_n—OCF₂ CF₂ CF₂—C(O)NH—CH₂ CH₂ CH₂—Si(OCH₃)₃  (3A)

Average of number n of units: 13, number average molecular weight of compound (3A): 4,920

Example 4

Compound (1-1C) was obtained in accordance with the method described in Preparation Example 15 of Japanese Patent No. 5761305.
CF₃(OCF₂ CF₂)₁₅(OCF₂)₁₆ OCF₂ CH₂ OCH₂ CH₂ CH₂ Si[CH₂ CH₂ CH₂ Si(OCH₃)₃]₃  (1-1C)

Mn of compound (1-1C): 3,600

Example 8

In accordance with Example 4 in JP-A-2015 —199906, compound (1-3B) was obtained.

[Figure (not displayed)]

In the above formula (1-3B), p1:q≈47:53, p1+q1=43.

Mn of compound (1-3B): 4,800