Synthesis of Allylbenzene Triphenylphosphine Derivatives

γ-cyclodextrin (γ-CD) and methyl β-cyclodextrin (M-β-CD) were purchased from Sigma Aldrich (St. Louis, MI, USA). Apiol, dillapiol, allyltetramethoxybenzene and myristicin were isolated from plant extracts as described earlier [77 (link)]. Heparin (MM 50–80 kDa), organic solvents, salts and acids were from Reakhim (Moscow, Russia).
The synthesis of triphenylphosphine derivatives of allylbenzenes was performed as described earlier in the work [46 (link)].

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Zlotnikov I.D., Krylov S.S., Semenova M.N., Semenov V.V, & Kudryashova E.V. (2023). Triphenylphosphine Derivatives of Allylbenzenes Express Antitumor and Adjuvant Activity When Solubilized with Cyclodextrin-Based Formulations. Pharmaceuticals, 16(12), 1651.

Publication 2023

γ-cyclodextrin (γ-CD) methyl β-cyclodextrin (M-β-CD)

Corresponding Organization : Lomonosov Moscow State University

Other organizations : N.D. Zelinsky Institute of Organic Chemistry, Koltzov Institute of Developmental Biology

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Variable analysis

independent variables

γ-cyclodextrin (γ-CD)
Methyl β-cyclodextrin (M-β-CD)
Apiol
Dillapiol
Allyltetramethoxybenzene
Myristicin
Triphenylphosphine derivatives of allylbenzenes

dependent variables

Not explicitly mentioned

control variables

Heparin (MM 50–80 kDa)
Organic solvents
Salts
Acids

positive controls

Not explicitly mentioned

negative controls

Not explicitly mentioned

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