Nitrile Reduction with Complex 2

A 25 mL round-bottom
flask containing 1.0 mmol of nitrile and Complex 2 (1.0
mol %) in DMSO (6 mL) was added. The reaction was monitored
by ATR-IR spectrum at 4 h intervals.

Partial Protocol Preview
This section provides a glimpse into the protocol.
The remaining content is hidden due to licensing restrictions, but the full text is available at the following link: Access Free Full Text.

Babu A, & Sinha A. (2024). Catalytic Tetrazole Synthesis via [3+2] Cycloaddition of NaN3 to Organonitriles Promoted by Co(II)-complex: Isolation and Characterization of a Co(II)-diazido Intermediate. ACS Omega, 9(19), 21626-21636.

Publication 2024

Corresponding Organization : Vellore Institute of Technology University

Top 5 similar protocols

Variable analysis

independent variables

Amount of nitrile (1.0 mmol)
Amount of Complex 2 (1.0 mol %)
Volume of DMSO (6 mL)

dependent variables

Reaction progress monitored by ATR-IR spectrum at 4 h intervals

control variables

Volume of the round-bottom flask (25 mL)

Annotations

This protocol is too short. Unable to provide accurate annotations

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Revolutionizing how scientists
search and build protocols!