Betulin Disuccinate Synthesis and Characterization

Betulin disuccinate (obtained in the laboratory according to the procedure described earlier [10 (link)]), succinic anhydride 99% (ACROS Organics, Geel, Belgium), toluene (STANLAB, Lublin, Poland), acetic anhydride (POCh S.A., Gliwice, Poland), glycerol ethoxylate (average M_n~1000) (Sigma Aldrich, St. Louis, MO, USA), DMSO (Chempur, Piekary Śl., Poland), trichloro acetic acid (Chempur, Piekary Śl., Poland), acetic acid (Chempur, Piekary Śl., Poland), Tris buffer, sulforhodamine, tetrahydrofuran (Chempur, Piekary Śl., Poland), and methylene chloride (Chempur, Piekary Śl., Poland) were used as supplied.

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Niewolik D., Bednarczyk-Cwynar B., Ruszkowski P., Dzido G, & Jaszcz K. (2022). Highly Branched Betulin Based Polyanhydrides for Self-Assembled Micellar Nanoparticles Formulation. International Journal of Molecular Sciences, 23(19), 11462.

Publication 2022

Betulin disuccinate succinic anhydride 99% toluene acetic anhydride glycerol ethoxylate DMSO trichloroacetic acid acetic acid Tris buffer tetrahydrofuran methylene chloride

Acetic acid Acetic anhydride Betulin Dmso Glycerol Methylene chloride Succinic anhydride Tetrahydrofuran Toluene Trichloroacetic acid Tris buffer

Corresponding Organization : Silesian University of Technology

Other organizations : Poznan University of Medical Sciences

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Variable analysis

independent variables

Betulin disuccinate (obtained in the laboratory according to the procedure described earlier [10 (link)])
Succinic anhydride 99% (ACROS Organics, Geel, Belgium)
Glycerol ethoxylate (average M_n~1000) (Sigma Aldrich, St. Louis, MO, USA)

dependent variables

Measured outcomes not explicitly mentioned

control variables

Toluene (STANLAB, Lublin, Poland)
Acetic anhydride (POCh S.A., Gliwice, Poland)
DMSO (Chempur, Piekary Śl., Poland)
Trichloroacetic acid (Chempur, Piekary Śl., Poland)
Acetic acid (Chempur, Piekary Śl., Poland)
Tris buffer
Sulforhodamine
Tetrahydrofuran (Chempur, Piekary Śl., Poland)
Methylene chloride (Chempur, Piekary Śl., Poland)

controls

Positive controls not explicitly mentioned
Negative controls not explicitly mentioned

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