Single crystals of racemic D6H were grown in CH 2 Cl 2 with the diffusion of a vapor of n-pentane. Typically, 5.0 mg of racemic D6H was dissolved in 1 mL of CH 2 Cl 2 , and a vapor of n-pentane was allowed to diffuse into the solution for 3 days. The resulting crystals were washed with n-pentane and then dried.
Protocol detail
Crystallization of Racemic D6H Compound
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Corresponding Organization : Zhejiang Sci-Tech University
Other organizations : Shanghai Jiao Tong University, ShanghaiTech University
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Variable analysis
independent variables
- Concentration of racemic D6H in CH2Cl2 (5.0 mg/1 mL)
- Duration of n-pentane vapor diffusion (3 days)
- Characteristics of the resulting single crystals (not explicitly mentioned)
- Solvent used (CH2Cl2)
- Vapor used for diffusion (n-pentane)
- Positive control: Not specified
- Negative control: Not specified
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