Immunoblotting of Native and Denatured Proteins
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Corresponding Organization : Columbia University Irving Medical Center
Protocol cited in 7 other protocols
Variable analysis
- Protein complexes from 3–12% precast Bis–Tris Native PAGE gels (Life Technologies)
- Thoraxes homogenized in radioimmunoprecipitation assay buffer (150-mM NaCl, 1% Triton X-100, 0.5% sodium deoxycholate, 0.1% SDS, and 50-mM Tris-HCl, pH 8) supplemented with Halt protease inhibitors (Pierce)
- Immunoreactivity detected by ECL and analyzed by a ChemiDoc Gel imaging system from Bio-Rad
- Polyvinylidene difluoride membranes (Bio-Rad) used for protein transfer
- Membranes blocked in 5% (wt/vol) nonfat dry milk in TBS for 30 min
- Membranes incubated in primary antibodies dissolved in 2% BSA and 0.1% Tween 20 in TBS (TBST) overnight at 4°C
- Membranes rinsed four times for 10 min each in 0.1% TBST
- Membranes blocked for 30 min in 5% (wt/vol) nonfat dry milk in TBST
- Membranes incubated for 2 h with HRP-conjugated secondary antibodies dissolved in 2% BSA and 0.1% TBST
- Membranes rinsed four times for 10 min each in 0.1% TBST
- Anti-NDUFS3 (Abcam, ab14711)
- Anti-ATPsynβ (Life Technologies, A-21351)
- Anti-VDAC1/Porin (Abcam, ab14734)
- Anti–cytochrome C (Abcam, ab13575)
- Anti-Hsp60 (Cell Signaling Technology, 4869S)
- Anti-Hsp90 (Cell Signaling Technology, 4874S)
- Rabbit polyclonal antibodies generated by Biomatik
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