Atom Transfer Radical Polymerization on CI Particles

N,N,N-Triethylamine (TEA, ≥ 99%), N,N,N′,N″,N″-pentamethyldiethylenetriamine
(PMDETA, 99%), copper(I)
bromide (CuBr, ≥ 99.999%), ethyl α-bromoisobutyrate (EBiB,
98%), α-bromoisobutyryl bromide (BiBB, 98%), 2-bromopropionitrile
(BPN, 97%), methyl 2-bromopropionate (MBP, 98%), monomer 2-(trimethylsilyloxy)ethyl
methacrylate (HEMATMS, 99%), N,N-dimethylformamide (DMF, 99%), anisole (99%), N,N-dimethylacetamide (DMAc, 99%), dimethyl sulfoxide (DMSO,
99.9%), anhydrous tetrahydrofuran (aTHF, 99.9%), acetone (99.5%),
tetrahydrofuran (THF, 99%), isohexane (≥99%), 3-(aminopropyl)triethoxysilane
(APTES, 97%), potassium fluoride (KF, 99%), and tetrabutylammonium
fluoride (TBAF, 1.0 M in THF) were purchased from Aldrich (USA). HEMATMS
monomer was purified by passing through a column filled with basic
alumina before use. All other listed reagents were used as received.
The CI particles (>97.8%) with average of 1 μm in diameter
(ES
grade, BASF, Germany) were used in this study. Silicone oil Lukosiol
M200 (Koln, Czech Republic) was used as received.

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Kozłowski S., Osička J., Ilcikova M., Galeziewska M., Mrlik M, & Pietrasik J. (2024). From Brush to Dendritic Structure: Tool for Tunable Interfacial Compatibility between the Iron-Based Particles and Silicone Oil in Magnetorheological Fluids. Langmuir, 40(10), 5297-5305.

Publication 2024

anisole dimethyl sulfoxide anhydrous tetrahydrofuran acetone tetrahydrofuran potassium fluoride

Corresponding Organization : Tomas Bata University in Zlín

Other organizations : Polymer Institute of the Slovak Academy of Sciences, Slovak Academy of Sciences

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Variable analysis

independent variables

N,N,N-Triethylamine (TEA, ≥ 99%)
N,N,N′,N″,N″-pentamethyldiethylenetriamine (PMDETA, 99%)
Copper(I) bromide (CuBr, ≥ 99.999%)
Ethyl α-bromoisobutyrate (EBiB, 98%)
α-bromoisobutyryl bromide (BiBB, 98%)
2-bromopropionitrile (BPN, 97%)
Methyl 2-bromopropionate (MBP, 98%)
Monomer 2-(trimethylsilyloxy)ethyl methacrylate (HEMATMS, 99%)
N,N-dimethylformamide (DMF, 99%)
Anisole (99%)
N,N-dimethylacetamide (DMAc, 99%)
Dimethyl sulfoxide (DMSO, 99.9%)
Anhydrous tetrahydrofuran (aTHF, 99.9%)
Acetone (99.5%)
Tetrahydrofuran (THF, 99%)
Isohexane (≥99%)
3-(aminopropyl)triethoxysilane (APTES, 97%)
Potassium fluoride (KF, 99%)
Tetrabutylammonium fluoride (TBAF, 1.0 M in THF)

dependent variables

Not explicitly mentioned

control variables

CI particles (>97.8%) with average of 1 μm in diameter (ES grade, BASF, Germany)
Silicone oil Lukosiol M200 (Koln, Czech Republic)

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