Synthesis and Characterization of PVA-Butanal Adduct

PVA (MW 24 000–24 500 g mol⁻¹, hydrolysis degree of 99.0%) and ethanol (99.5%) were supplied by Shanghai Macklin Biochemical Co., Ltd. n-Butanal (99.5%) was got from Shanghai Mairuier Chemical Technology Co., Ltd. Benzyltrimethylammonium chloride (BAC, 98.0%) was got from Shanghai Di Bo Chemical Co., Ltd. p-Toluenesulfonic acid monohydrate (PTSA, 99.0%) was got from Shanghai Aladdin Biochemical Technology Co., Ltd. Sodium dodecyl sulfonate (SDS, 97.0%) and sodium hydroxide (NaOH, 98.0%) was supplied by Sinopharm Chemical Reagent Co., Ltd. Hydrochloric acid (HCl, 36–38%) and hydroxylamine hydrochloride (98.5%) were bought from Shanghai Titan Scientific Co., Ltd.

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Luan W., Sun L., Zeng Z, & Xue W. (2023). Optimization of a polyvinyl butyral synthesis process based on response surface methodology and artificial neural network. RSC Advances, 13(11), 7682-7693.

Publication 2023

PVA ethanol Sodium dodecyl sulfonate sodium hydroxide Hydrochloric acid

Acid Benzyltrimethylammonium chloride Butanal Ethanol Hydrochloric acid Hydrolysis Hydroxylamine hydrochloride Ptsa Sodium Sodium hydroxide Sulfonate

Corresponding Organization : East China University of Science and Technology

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Variable analysis

independent variables

PVA (MW 24 000–24 500 g mol^-1, hydrolysis degree of 99.0%)
Ethanol (99.5%)
N-Butanal (99.5%)
Benzyltrimethylammonium chloride (BAC, 98.0%)
P-Toluenesulfonic acid monohydrate (PTSA, 99.0%)
Sodium dodecyl sulfonate (SDS, 97.0%)
Sodium hydroxide (NaOH, 98.0%)
Hydrochloric acid (HCl, 36–38%)
Hydroxylamine hydrochloride (98.5%)

dependent variables

Not explicitly mentioned

control variables

Not explicitly mentioned

positive controls

No positive controls mentioned

negative controls

No negative controls mentioned

Annotations

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