Synthesis of PVDF-HFP Electrolyte Membrane

Poly(vinylidene fluoride-co-hexafluoropropylene) (Mw ~400,000) is purchased from Sigma Aldrich. Succinonitrile (SN), N, N-Dimethylformamide (DMF), lithium trifluoromethanesulfonate (LiOTF), Zinc trifluoromethanesulfonate (Zn(OTF)₂), Methyl acrylate (MA) and 2,2’-Azobis(2-methylpropionitrile) (AIBN) are purchased from Aladdin. MA was vacuum-distilled to remove the inhibitor. AIBN was recrystallized before use. Methacryl polyhedral oligomeric silsesquioxane cage mixture (POSS) was purchased from Forsman.

Free full text: Click here

Chen Z., Wang T., Wu Z., Hou Y., Chen A., Wang Y., Huang Z., Schmidt O.G., Zhu M., Fan J, & Zhi C. (2024). Polymer hetero-electrolyte enabled solid-state 2.4-V Zn/Li hybrid batteries. Nature Communications, 15, 3748.

Publication 2024

Corresponding Organization :

Other organizations : City University of Hong Kong, Chemnitz University of Technology

Top 5 similar protocols

Variable analysis

independent variables

Poly(vinylidene fluoride-co-hexafluoropropylene) (Mw ~400,000) concentration
Succinonitrile (SN) concentration
Lithium trifluoromethanesulfonate (LiOTF) concentration
Zinc trifluoromethanesulfonate (Zn(OTF)2) concentration
Methyl acrylate (MA) concentration
2,2'-Azobis(2-methylpropionitrile) (AIBN) concentration
Methacryl polyhedral oligomeric silsesquioxane cage mixture (POSS) concentration

dependent variables

Measured outcomes not explicitly mentioned

control variables

Vacuum distillation of MA to remove inhibitor
Recrystallization of AIBN before use

Annotations

Based on most similar protocols

Etiam vel ipsum. Morbi facilisis vestibulum nisl. Praesent cursus laoreet felis. Integer adipiscing pretium orci. Nulla facilisi. Quisque posuere bibendum purus. Nulla quam mauris, cursus eget, convallis ac, molestie non, enim. Aliquam congue. Quisque sagittis nonummy sapien. Proin molestie sem vitae urna. Maecenas lorem.

As authors may omit details in methods from publication, our AI will look for missing critical information across the 5 most similar protocols.

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Revolutionizing how scientists
search and build protocols!