Synthesis and Characterization of Perovskite Solar Cell Materials

MAI (CH₃NH₃I) was synthesized from CH₃NH₂ and HI based on the reported literature44 (link). Lead acetate (Pb(Ac)₂) was purchased from Sigma Aldrich and was dehydrated before use45 (link). Poly(3,4-ethylenedioxythiophene):poly(styrenesulfonate) (PEDOT:PSS, PVP AI4083) was purchased from Heraeus Clevios. [6,6]-phenyl C₆₁-butyric acid methyl ester (PC₆₁BM) was purchased from C-Nano Tech. 2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline was purchased from Alfa Aesar. All the liquid reagents, including DMF, chlorobenzene (CB) and chloroform (CF) were purchased from Acros and used as received.

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Hu Q., Zhao L., Wu J., Gao K., Luo D., Jiang Y., Zhang Z., Zhu C., Schaible E., Hexemer A., Wang C., Liu Y., Zhang W., Grätzel M., Liu F., Russell T.P., Zhu R, & Gong Q. (2017). In situ dynamic observations of perovskite crystallisation and microstructure evolution intermediated from [PbI6]4− cage nanoparticles. Nature Communications, 8, 15688.

Publication 2017

Lead acetate (Pb(Ac)2) 2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline DMF chlorobenzene chloroform

Chlorobenzene Chloroform Diphenyl Ester Lead acetate Phenanthroline Phenyl acid Poly Poly styrenesulfonate

Corresponding Organization :

Other organizations : Peking University, Lawrence Berkeley National Laboratory, University of Surrey, École Polytechnique Fédérale de Lausanne, Collaborative Innovation Center of Quantum Matter, Shanxi University

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Variable analysis

independent variables

CH3NH2 and HI used to synthesize MAI (CH3NH3I)
Lead acetate (Pb(Ac)2) purchased and dehydrated before use

dependent variables

Synthesized MAI (CH3NH3I)

control variables

Poly(3,4-ethylenedioxythiophene):poly(styrenesulfonate) (PEDOT:PSS, PVP AI4083) purchased from Heraeus Clevios
[6,6]-phenyl C61-butyric acid methyl ester (PC61BM) purchased from C-Nano Tech
2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline purchased from Alfa Aesar
Liquid reagents DMF, chlorobenzene (CB) and chloroform (CF) purchased from Acros and used as received

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