Synthesis and Characterization of Nanoparticles

All solvents and reagents used were of the highest analytical reagent grade and were not purified further. The melting points were determined using the Stuart Scientific SMP1 and uncorrected. TLC was performed on UV fluorescent Silica gel Merck 60 F254 plates, with spots identified using a UV lamp (254 nm). The main functional groups were identified using a SHIMADZU FTIR~Affinity~1S spectrometer with a range of 400~4000 cm⁻¹. NMR spectra were collected using a Bruker spectrometer (400 MHz) with tetramethyl silane (TMS) as an internal reference. The LCMS/MS impact II was used for high-resolution mass spectroscopy (HRMS). Elemental analyses were carried out using a Vario EL III Elementar Analyzer. The nanoparticles used in this investigation were prepared according to our previous study [31 (link)].