Synthesis and Characterization of a Calix[4]arene Derivative
Corresponding Organization :
Other organizations : Delft University of Technology, Centre de Biophysique Moléculaire, Le Studium
Protocol cited in 31 other protocols
Variable analysis
- Modifications to the lower rim of the calix[4]arene backbone, including propylation (7a,b) of the hydroxylic groups and condensation of one of the hydroxyls (8a) with N-(3-bromo)propylphthalimide
- Nitration (9a,b) of the upper rim of the calix[4]arene backbone
- Reduction (10a,b) of the nitro groups to the amines
- Luminescence measurements, including qualitative measurements on a Jasco J815 CD spectrometer and quantitative measurements on a Horiba-Jobin-Yvon Fluorolog 3 spectrofluorimeter
- Luminescence lifetimes of Tb(III) complexes
- Quantum yields measured using an integration sphere
- Nile red fluorescence measurements, including the determination of the maximum emission wavelength (λmax) as a function of calix[4]arene concentration
- All reagents and anhydrous solvents used during the synthesis were of commercial quality
- Experimental conditions, such as temperature (25°C) and HPLC operating conditions (40°C)
- None explicitly mentioned
- None explicitly mentioned
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