Example 10
Compound I Form F was obtained via slurry of Compound I calcium salt hydrate Form A in MEK at room temperature.
A. X-Ray Powder Diffraction
XRPD was performed with a Panalytical X'Pert3 Powder XRPD on a Si zero-background holder. The 20 position was calibrated against a Panalytical Si reference standard disc. The XRPD diffractogram for Compound I Form F is shown in
Compound I Form F is characterized by the following elemental analysis Table:
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