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Multianalytical Characterization of MnFe2O4 Composites

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The MnFe₂O₄ phase on silica and GO was analyzed using high-angle XRD instrument (Miniflex 600, Rigaku, Tokyo, Japan). The textural features of two supports were measured using the N₂ adsorption technique (ASAP-2020 plus, Micromeritics, Norcross, GA, USA). The morphological variations of manganese ferrite nanoparticles over the silica and GO support was investigated using transmission electron microscopy (TEM, JEM2100F, JEOL, Tokyo, Japan). The sample preparation procedure was described in our previous publication [14 (link)]. The superparamagnetic properties of the two composites were analyzed using vibrating sample magnetometer (VSM), LDJ electronics, 9600, Troy MI, USA. The ferrite nanoparticle chemical coordination was analyzed using DRS-UV-visible spectroscopy analysis (JASCO V-750, Tokyo, Japan).

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Almohazey D., Ravinayagam V., Alamoudi W., Akhtar S., Dafalla H., AlSuwaidan H.N., Almutairi S.T., Alghamdi H.S., Aldamen S.A., Almessiere M.A., Baykal A., Maarouf A.A, & Jermy B.R. (2023). Insights of Platinum Drug Interaction with Spinel Magnetic Nanocomposites for Targeted Anti-Cancer Effect. Cancers, 15(3), 695.

Publication 2023

Miniflex 600 ASAP-2020 plus JEM2100F V-750

Adsorption Ferrite Manganese ferrite Silica Spectroscopy Transmission electron microscopy

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Variable analysis

independent variables

MnFe2O4 phase on silica and GO

dependent variables

Textural features of two supports
Morphological variations of manganese ferrite nanoparticles over the silica and GO support
Superparamagnetic properties of the two composites
Ferrite nanoparticle chemical coordination

control variables

Sample preparation procedure (described in previous publication)

controls

No positive or negative controls were explicitly mentioned.

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