Fabrication of Hydrogel Tubes for Tissue Engineering
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Corresponding Organization : University of Miami
Other organizations : University of Michigan–Ann Arbor
Variable analysis
- Crosslinking of 20% w/v 8-arm polyethylene glycol maleimide (PEG-MAL, 20 kDa) with 5 mM slow-degrading-plasmin-sensitive YKND cross-linking peptide (Ac-GCYKNDGCYKNDCG)
- Homogenization speed and duration (4000 rpm for 1 minute) during water-oil emulsion to form microspheres
- Concentration of Irgacure 2959 photoinitiator dissolved in N-vinylpyrrolidinone (1% w/v)
- Duration of UV exposure (3 minutes) to initiate free radical polymerization
- Diameter of microspheres (ranging between 15 and 150 μm with an average of 45 μm)
- Dimensions of PEG tubes (approximate OD: 600 μm, ID: 250 μm, porosity 66%)
- Material composition of PEG-MAL (20 kDa) and cross-linking peptide (Ac-GCYKNDGCYKNDCG)
- Silicone oil (Fisher, Hampton, NH) with 2% Tween-20 (Sigma, St. Louis, MO) used for water-oil emulsion
- PDMS (Dow Corning, Midland, MI) molds used to generate PEG tubes
- Not explicitly mentioned
- Not explicitly mentioned
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